1,3-Bis(isocyanatomethyl)benzene

  • Name:1,3-Bis(isocyanatomethyl)benzene
  • CAS:3634-83-1
  • Purity:99%
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Details

Reputable supplier selling 1,3-Bis(isocyanatomethyl)benzene 3634-83-1 with stock

  • Molecular Formula:C10H8N2O2
  • Molecular Weight:188.186
  • Vapor Pressure:0.021Pa at 20℃ 
  • Melting Point:-7 °C 
  • Refractive Index:n20/D 1.451  
  • Boiling Point:293.7 °C at 760 mmHg 
  • Flash Point:119.1 °C 
  • PSA:58.86000 
  • Density:1.11 g/cm3 
  • LogP:1.35820 

1,3-Bis(isocyanatomethyl)benzene(Cas 3634-83-1) Usage

Flammability and Explosibility

Nonflammable

Safety Profile

Moderately toxic by ingestion. A severe skin and eye irritant. A sensitizer. A flammable liquid. When heated to decomposition it emits very toxic fumes of NOx. See also ISOCYANATES.

InChI:InChI=1/C8H8N2O2/c11-9-5-7-2-1-3-8(4-7)6-10-12/h1-4H,5-6H2

3634-83-1 Relevant articles

DIISOCYANATE COMPOSITION, PREPARATION METHOD THEREOF AND OPTICAL MATERIAL USING SAME

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Paragraph 0212-0215; 0243-0246; 0274-0277; 0280-0282, (2021/06/11)

The diisocyanate composition according t...

METHOD OF PREPARING DIISOCYANATE COMPOSITION AND OPTICAL LENS

-

Paragraph 0175-0179; 0195-0199; 0218-0221, (2021/06/11)

In the embodiments, an aqueous hydrochlo...

Construction of unsymmetrical bis-urea macrocyclic host for neutral molecule and chloride-ion binding

Bhuyan, Deepak,Guha, Samit,Mukherjee, Ayan,Paul, Biprajit

supporting information, (2021/06/27)

Construction of synthetic macrocyclic ho...

METHOD OF PREPARING DIISOCYANATE COMPOSITION

-

Paragraph 0219-0226; 0243-0245; 0252-0254; 0277-0279, (2021/06/11)

In the embodiments, an aqueous hydrochlo...

3634-83-1 Process route

1,3-di(aminomethyl)benzene
1477-55-0

1,3-di(aminomethyl)benzene

bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

m-xylylene diisocyanate
3634-83-1,53208-23-4

m-xylylene diisocyanate

Conditions
Conditions Yield
1,3-di(aminomethyl)benzene; With hydrogenchloride; In chlorobenzene; at 60 - 65 ℃; for 1h;
bis(trichloromethyl) carbonate; With hydrogenchloride; triphenylphosphine; In chlorobenzene; at 132 ℃; Solvent; Temperature;
94.8%
1,3-di(aminomethyl)benzene; With hydrogenchloride; In water; at 10 - 60 ℃; for 2h; Large scale;
bis(trichloromethyl) carbonate; In 1,2-dichloro-benzene; at 130 ℃; for 28h; Temperature; Large scale;
94%
1,3-di(aminomethyl)benzene; With hydrogenchloride; In water; at 50 ℃; for 1h;
bis(trichloromethyl) carbonate; In 1,2-dichloro-benzene; at 130 ℃; Temperature;
90%
With triethylamine; In dichloromethane; at 25 ℃; for 2h; Inert atmosphere;
88%
With chloro-trimethyl-silane; triethylamine; In chlorobenzene; at -15 - 132 ℃; for 4h; Solvent; Temperature; Time; Reagent/catalyst; Inert atmosphere;
85.24%
1,3-di(aminomethyl)benzene; With hydrogenchloride; In water; at 60 ℃; for 1h;
bis(trichloromethyl) carbonate; In 1,2-dichloro-benzene; at 125 ℃; for 28h;
1,3-di(aminomethyl)benzene; With hydrogenchloride; In water; at 60 ℃; for 1h;
bis(trichloromethyl) carbonate; In 1,2-dichloro-benzene; at 125 ℃; for 28h; Solvent;
[3-(Phenoxycarbonylamino-methyl)-benzyl]-carbamic acid phenyl ester
16578-54-4

[3-(Phenoxycarbonylamino-methyl)-benzyl]-carbamic acid phenyl ester

m-xylylene diisocyanate
3634-83-1,53208-23-4

m-xylylene diisocyanate

Conditions
Conditions Yield
With DURANATE TPA-100; In 1,2-dichloro-benzene; at 250 ℃; for 200h; under 6000.6 Torr; Inert atmosphere;
85%
In 1,2-dichloro-benzene; at 160 - 250 ℃; under 6000.6 Torr; Inert atmosphere;
82%

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    1,3-Bis<(1-carboxymethyl-3-hydantoinyl)methyl>benzene

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